毒素检测报告(饮用水)
项目报告
1 样品信息Sample description
收到饮用水样品xx个,a和b
A total of xx drinking water samples, where received by the customer.
2 材料与方法Materials and Methods
2.1 试剂Chemicals
所有的溶剂与试剂均为色谱级,微囊藻毒素YR,微囊藻毒素LR,微囊藻毒素RR标准品购于xxx
All chemicals and solvent were HPLC. Standard: microcystin YR, microcystin LR, microcystin RR and were purchased from xxx.
2.2 样品处理Sample Preparation
1) 将样品摇匀, 经过全自动固相萃取仪的富集程序;
2) 40℃氮气吹干,洗脱液定容至1 mL,并用0.22 µm滤膜过滤,进样10 µL。
2.3 HPLC分析HPLC Analysis
本实验所用的仪器为Agilent高效液相色谱仪,配备二极管阵列检测器。
色谱柱为xxx C18 (250 mm*4.6 mm, 5 μm),流动相为xxx缓冲液-甲醇(43 : 57, V/V),流速为0.9 mL/min,柱温为xx℃。
3 结果Results
色谱图Chromatogram
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